3-Ethyl­sulfinyl-2-(4-fluoro­phen­yl)-5-iodo-1-benzofuran

نویسندگان

  • Hong Dae Choi
  • Pil Ja Seo
  • Byeng Wha Son
  • Uk Lee
چکیده

In the title compound, C(16)H(12)FIO(2)S, the 4-fluoro-phenyl ring is rotated slightly out of the benzofuran plane, as indicated by the dihedral angle of 4.48 (5)°. In the crystal structure, pairs of I⋯O halogen bonds [I⋯O = 3.123 (1) Å] link the mol-ecules into centrosymmetric dimers. These dimers are further linked via aromatic π-π inter-actions between the benzene and 4-fluoro-phenyl rings of neighbouring mol-ecules [centroid-centroid distance = 3.620 (3) Å].

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منابع مشابه

3-Ethyl­sulfinyl-2-(4-fluoro­phen­yl)-5-iodo-7-methyl-1-benzofuran

In the title compound, C(17)H(14)FIO(2)S, the 4-fluoro-phenyl ring is rotated out of the benzofuran plane, as indicated by the dihedral angle of 15.60 (6)°. The crystal structure exhibits an I⋯O inter-action [3.052 (2) Å].

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3-Ethyl­sulfinyl-2-(3-fluoro­phen­yl)-5-iodo-7-methyl-1-benzofuran

In the title compound, C(17)H(14)FIO(2)S, the 3-fluoro-phenyl ring makes a dihedral angle of 14.56 (5)° with the mean plane [r.m.s. deviation = 0.012 (1) Å] of the benzofuran fragment. In the crystal, mol-ecules are linked via pairs of I⋯O contacts [3.038 (2) Å], forming inversion dimers. In the 3-fluoro-phenyl ring, the F atom is disordered over two positions, with site-occupancy factors of 0....

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5-Chloro-3-ethyl­sulfinyl-2-(4-fluoro­phen­yl)-7-methyl-1-benzofuran

In the title compound, C(17)H(14)ClFO(2)S, the 4-fluoro-phenyl ring is rotated slightly out of the benzofuran plane, as indicated by the dihedral angle of 8.32 (5)°. The crystal structure features a short Cl⋯O contact [3.092 (1) Å].

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5-Chloro-3-ethyl­sulfinyl-2-(4-fluoro­phen­yl)-1-benzofuran

In the title compound, C(16)H(12)ClFO(2)S, the 4-fluoro-phenyl ring is rotated out of the benzofuran plane, as indicated by the dihedral angle of 6.96 (5)°. The crystal structure exhibits a Cl⋯O inter-action with a Cl⋯O distance of 3.163 (1) Å.

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5-Bromo-3-ethyl­sulfinyl-2-(4-fluoro­phen­yl)-7-methyl-1-benzofuran

In the title compound, C(17)H(14)BrFO(2)S, the 4-fluoro-phenyl ring is rotated slightly out of the benzofuran plane, making a dihedral angle of 7.60 (4)°. The crystal structure is stabilized by a Br⋯O halogen-bonding inter-action [3.048 (1) Å].

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عنوان ژورنال:

دوره 66  شماره 

صفحات  -

تاریخ انتشار 2010